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1 article(s) from Löbbicke, Ruben

First examples of organosilica-based ionogels: synthesis and electrochemical behavior

Andreas Taubert,
Ruben Löbbicke,
Barbara Kirchner and
Fabrice Leroux

Beilstein J. Nanotechnol. 2017, 8, 736–751, doi:10.3762/bjnano.8.77

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Figure 1: Ball-and-stick representation of the simulation box. Visualized with TRAVIS [43] and vmd [44]. Left: cation...

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Figure 2: Representative photographs and TEM images of organosilica monoliths. (A) Wet TBM20 after Soxhlet ex...

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Figure 3: Carbon, hydrogen, and nitrogen contents of silica monoliths made from methanol (A) and acetone (B).

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Figure 4: TGA data of pure organosilica monoliths.

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Figure 5: Representative IR spectra of TBA40 and MBA40.

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Figure 6: (A) SAXS pattern of TBA40 and (B) nitrogen sorption data of TBA20 to TBA60.

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Scheme 1: Synthesis of the IL [BmimSO₃H][PTS].

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Figure 7: Photograph of an IG resulting from the combination of the TBA60 organosilica matrix and [BmimSO₃H][...

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Figure 8: IR spectra of a neat TBA20 monolith, pure IL, and the resulting TBA20IL IG.

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Figure 9: EA data of IGs. Samples shown in panel (A) were made via the methanol-based synthesis and samples s...

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Figure 10: TGA data of MBA20IL, MBA40IL, MBA50IL, and MBA60IL along with TGA trace obtained from wet MBA60IL o...

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Figure 11: DSC heating traces of (A) [BmimSO₃H][PTS] and (B) the resulting TBA IGs. Gray areas highlight the r...

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Figure 12: Nyquist curve Z”(ω) vs Z’(ω) for TBA20IL with zoom-ins to the central areas of the plot vs temperat...

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Figure 13: Variation of log(σ·T) versus 1000/T for all IGs. The change in the energy of activation likely does...

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Figure 14: Variation of (A) tan δ vs log f and (B) relaxation time vs 1000/T for MBA40. The temperature is as ...

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Figure 15: Full temporal development (from equilibrium search to production run) of all 32 intramolecular O–H ...

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Figure 16: Combined distribution function of the intramolecular O–H distances (including only the bonding oxyg...

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Full Research Paper

Published 29 Mar 2017

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